During my DevOps interview with Nioyatech, the process started with an initial screening by a recruiter who discussed my experience in cloud infrastructure and automation tools like AWS, Jenkins, Docker, and Kubernetes. This was followed by a technical round where I was asked to solve hands-on tasks such as setting up a CI/CD pipeline, troubleshooting infrastructure issues, and optimizing system performance. The interview also included questions on infrastructure as code, particularly focusing on my experience with Terraform and Ansible.